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. Author manuscript; available in PMC: 2018 Dec 13.
Published in final edited form as: J Am Chem Soc. 2017 Dec 4;139(49):18101–18106. doi: 10.1021/jacs.7b10907

Table 3.

Scope with respect to the electrophile.

graphic file with name nihms978053u4.jpg
entry electrophile yield (%)a
1 graphic file with name nihms978053t2.jpg 81
2 graphic file with name nihms978053t3.jpg 70
3 graphic file with name nihms978053t4.jpg 72
4 graphic file with name nihms978053t5.jpg 56
5 graphic file with name nihms978053t6.jpg 49 (74)b
6 graphic file with name nihms978053t7.jpg 81
7 graphic file with name nihms978053t8.jpg 88
8 graphic file with name nihms978053t9.jpg 81
9c graphic file with name nihms978053t10.jpg 85
a

Yield of purified product (average of two experiments).

b

Yield of purified product when a Hg lamp is used.

c

Starting material: 1:5.4 cis/trans; product: 6.5:1 cis/trans.