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. 2017 Aug 16;2(8):4604–4611. doi: 10.1021/acsomega.7b00834

Table 1. Independent Variables in the Measurementsa.

part I
part II
part III
curing conditions
processing
polymer composition
samples 1A samples 1B samples 2A samples 2B samples 3A samples 3B
31 mol % TCMDA 31 mol % TCMDA 31 mol % TCMDA 31 mol % TCMDA 10, 20, 31, 45, 50 mol % TCMDA 10, 31, 50 mol % TCMDA
spin-coated spin-coated casted spin-coated spin-coated casted
365 nm 254 nm 365 nm 365 nm 365 nm 365 nm
30, 60, 120 min 30, 60, 120 min 120 min 120 min 60 min 60 min
a

Part I of the study tested how differences in the curing wavelength, as well as exposure to UV light during the polymerization process, affected the Tg. Part II tested the differences in the polymer characteristics when casted compared with when spin-coated. Part III examined how monomer mole variations affect Tg, the degradation process, and water uptake. Samples 3A and 3B were not tested against each other, but against themselves.