Skip to main content
. 2017 Jul 12;2(7):3494–3501. doi: 10.1021/acsomega.7b00417

Table 1. NMR Data of Anomoian B (1) in CD3OD and Aplyzanzine B (2) in CDCl3.

1
2
pos. δC type δHm (J in Hz) pos. δC type δHm (J in Hz)
1 134.5 C   1 133.4 C  
2 135.2 CH 7.51s 2 133.6 CH 7.40s
3 119.3 C   3 118.5 C  
4 155.1 C   4 153.9 C  
5 119.3 C   5 118.5 C  
6 135.2 CH 7.51s 6 133.6 CH 7.40s
7 34.3 CH2 3.36m 7 34.1 CH2 3.22dd (12.4, 3.6)
    3.00m     3.09dd (12.4, 11.3)
8 70.5 CH 3.91dd (11.2, 4.6) 8 60.4 CH 4.97dd (11.3, 3.6)
9 167.2 C   9 166.8 C  
10 38.0 CH2 3.51m 10 54.9 CH2 5.06d (17.5)
    3.28m     4.19d (17.5)
11 30.6 CH2 1.84m 11 189.3 C  
    1.70m 12 132.5 C  
12 71.6 CH2 3.87m 13 132.7 CH 8.03s
    3.75m 14 118.9 C  
13 153.4 C   15 157.0 C  
14 119.4 C   16 118.9 C  
15 134.4 CH 7.57s 17 132.7 CH 8.03s
16 135.1 C   18 69.9 CH2 4.13t (5.5)
17 134.4 CH 7.57s 19 25.3 CH2 2.32dq (11.2, 5.5)
18 119.4 C   20 55.5 CH2 3.42m
19 30.3 CH2 2.99m 21 40.0 CH3 2.97s
20 59.1 CH2 3.33m 22 40.0 CH3 2.97s
21 42.5 CH3 2.99s 23 42.9 CH3 2.88s
22 42.5 CH3 2.99s 24 42.9 CH3 2.88s
23 43.6 CH3 2.93s 25 60.7 CH3 3.85s
24 43.6 CH3 2.93s 26 37.6 CH3 2.75s
25 61.1 CH3 3.77s