Fig. 6. (a) Powder X-ray diffraction peak evolution for 1(Pd) (8.0–12.5°) showing in situ dehydration and SCO as a function of temperature. (b) Comparison of powder X-ray diffraction data (2–15°) for 1(Pd)·2H2O (at 200 and 95 K) and 1(Pd) (at 300 and 150 K), highlighting structural changes, peak broadening, and peak overlap with guest removal and SCO.
