Table 2.
1H- (600 MHz) and 13C- (150 MHz) NMR data of compound 18 in CD3OD
| Position | δH (int., mult., J in Hz) | δC |
|---|---|---|
| 1 | 6.00 (1H, s) | 80.4 |
| 2 | – | 194.6 |
| 3 | 5.27 (1H, s) | 126.5 |
| 4 | – | 164.0 |
| 5 | 3.33 (1H, m) | 49.7 |
| 6a 6b |
3.24 (1H, dd, 12.9, 3.6) 2.50 (1H, dd, 12.9, 6.6) |
25.6 |
| 7 | – | 122.4 |
| 8 | 5.00 (1H, m) | 79.0 |
| 9a 9b |
2.52 (1H, m) 0.90 (1H, t, 7.2) |
43.1 |
| 10 | – | 44.2 |
| 11 | – | 163.0 |
| 12 | – | 172.0 |
| 13 | 1.87 (3H, s) | 8.4 |
| 14 | 1.09 (3H, s) | 12.3 |
| 15 | 2.09 (3H, s) | 22.0 |
| 1′ | – | 176.8 |
| 2′ | 2.19 (3H, s) | 20.6 |