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. 2015 Jul 31;6(11):6147–6157. doi: 10.1039/c5sc02155c

Table 1. Compounds selected for soaking into NK1 apo crystals. Piperazine-like compounds with a sulphonic acid group and their binding constants obtained using SPR and NMR.

Piperazine-like compounds Structure K D in SPR a [mM] K D in NMR a [mM]
HEPES graphic file with name c5sc02155c-u1.jpg 2.4 ± 0.4 3.3 ± 0.4
(H)EPPS graphic file with name c5sc02155c-u2.jpg 7.0 ± 1.0 4.4 ± 1.8
PIPES graphic file with name c5sc02155c-u3.jpg 26.6 ± 0.6 45.9 ± 4.7
MES graphic file with name c5sc02155c-u4.jpg 24.3 ± 3.1 13.4 ± 5.7
MOPS graphic file with name c5sc02155c-u5.jpg 7.0 ± 1.0 4.7 ± 1.7
CHES graphic file with name c5sc02155c-u6.jpg 30.2 ± 3.1 15.7 ± 4.5
CAPS graphic file with name c5sc02155c-u7.jpg 1.2 ± 0.2 1.4 ± 0.5

aSteady-state binding constants.