Table 6.

Freeze drying recipe used for 3% w/v mannitol solution.

	1	2	3	4	5	6	7	8
Freezing step
Shelf setpoint [°C]	20	20	5	5	−5	−5	−45	−45
Time [min]	0	10	0	90	30	90	180	120
Primary drying
Shelf setpoint [°C]	−45	20	20
Time [min]	5	60	1800
Vaccum setpoint [mTorr]	60	60	60