Table 7.

Freeze drying recipe used for pure water.

	1	2	3	4	5	6	7	8
Freezing step
Shelf setpoint [°C]	20	20	5	5	−5	−5	−45	−45
Time [min]	0	10	0	90	30	90	180	120
Primary drying
Shelf setpoint [°C]	−45	−10	−50	−50
Time [min]	15	180	0	9999
Vaccum setpoint [mTorr]	60	60	60	60