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. 2018 Jul 5;2018:8478152. doi: 10.1155/2018/8478152

Table 2.

Selected bond lengths (Å) and bond angles (°) for complexes 1, 2, and 3.

Complex 1
Ni(1)–O(3) 1.990(2) Ni(1)–N(1) 1.991(3) Ni(1)–O(1) 2.068(3)
Ni(1)–N(3) 2.075(3) Ni(1)–N(2) 2.116(3) Ni(1)–O(4) 2.117(3)
O(3)–Ni(1)–N(1) 92.43(11) O(3)–Ni(1)–O(1) 173.63(10) N(1)–Ni(1)–O(1) 81.29(11)
O(3)–Ni(1)–N(3) 93.55(11) N(1)–Ni(1)–N(3) 172.77(11) O(1)–Ni(1)–N(3) 92.64(11)
O(3)–Ni(1)–N(2) 91.84(11) N(1)–Ni(1)–N(2) 96.26(12) O(1)–Ni(1)–N(2) 87.84(10)
N(3)–Ni(1)–N(2) 79.50(12) O(3)–Ni(1)–O(4) 89.99(11) N(1)–Ni(1)–O(4) 92.72(11)
O(1)–Ni(1)–O(4) 91.34(11) N(3)–Ni(1)–O(4) 91.33(11) N(2)–Ni(1)–O(4) 170.75(11)

Complex 2
Ni(1)–N(1) 1.987(3) Ni(1)–O(3) 1.997(3) Ni(1)–O(1) 2.068(3)
Ni(1)–N(3) 2.083(3) Ni(1)–O(4) 2.100(3) Ni(1)–N(2) 2.129(3)
N(1)–Ni(1)–O(3) 89.99(12) N(1)–Ni(1)–O(1) 81.80(12) O(3)–Ni(1)–O(1) 171.26(10)
N(1)–Ni(1)–N(3) 175.09(12) O(3)–Ni(1)–N(3) 94.34(11) O(1)–Ni(1)–N(3) 93.75(11)
N(1)–Ni(1)–O(4) 90.64(13) O(3)–Ni(1)–O(4) 92.52(12) O(1)–Ni(1)–O(4) 90.56(12)
N(3)–Ni(1)–O(4) 91.50(13) N(1)–Ni(1)–N(2) 98.70(12) O(3)–Ni(1)–N(2) 90.17(11)
O(1)–Ni(1)–N(2) 88.13(11) N(3)–Ni(1)–N(2) 78.99(12) O(4)–Ni(1)–N(2) 170.29(12)

Complex 3
Ni(1)–N(1) 2.000(6) Ni(1)–O(3) 2.003(5) Ni(1)–O(1) 2.053(5)
Ni(1)–N(3) 2.076(6) Ni(1)–N(2) 2.131(6) Ni(1)–O(5) 2.146(5)
Ni(2)–N(4) 1.982(6) Ni(2)–O(8) 1.992(5) Ni(2)–O(6) 2.059(5)
Ni(2)–N(6) 2.075(7) Ni(2)–O(10) 2.113(5) Ni(2)–N(5) 2.116(6)
Ni(3)–N(7) 1.995(7) Ni(3)–O(13) 2.008(5) Ni(3)–O(11) 2.056(6)
Ni(3)–N(8) 2.084(7) Ni(3)–O(15) 2.099(6) Ni(3)–N(9) 2.114(7)
N(1)–Ni(1)–O(3) 92.3(2) N(1)–Ni(1)–O(1) 82.0(2) O(3)–Ni(1)–O(1) 173.3(2)
N(1)–Ni(1)–N(3) 169.9(2) O(3)–Ni(1)–N(3) 93.2(2) O(1)–Ni(1)–N(3) 92.9(2)
N(1)–Ni(1)–N(2) 92.6(2) O(3)–Ni(1)–N(2) 96.1(2) O(1)–Ni(1)–N(2) 87.8(2)
N(3)–Ni(1)–N(2) 78.4(2) N(1)–Ni(1)–O(5) 95.3(2) O(3)–Ni(1)–O(5) 90.31(18)
O(1)–Ni(1)–O(5) 86.70(19) N(3)–Ni(1)–O(5) 93.2(2) N(2)–Ni(1)–O(5) 169.7(2)
N(4)–Ni(2)–O(8) 92.7(2) N(4)–Ni(2)–O(6) 81.3(2) O(8)–Ni(2)–O(6) 174.0(2)
N(4)–Ni(2)–N(6) 171.7(2) O(8)–Ni(2)–N(6) 93.3(2) O(6)–Ni(2)–N(6) 92.7(2)
N(4)–Ni(2)–O(10) 93.9(2) O(8)–Ni(2)–O(10) 90.41(19) O(6)–Ni(2)–O(10) 89.3(2)
N(6)–Ni(2)–O(10) 91.6(2) N(4)–Ni(2)–N(5) 95.0(2) O(8)–Ni(2)–N(5) 90.8(2)
O(6)–Ni(2)–N(5) 90.5(2) N(6)–Ni(2)–N(5) 79.3(3) O(10)–Ni(2)–N(5) 170.9(3)
N(7)–Ni(3)–O(13) 91.9(2) N(7)–Ni(3)–O(11) 80.3(3) O(13)–Ni(3)–O(11) 171.9(2)
N(7)–Ni(3)–N(8) 169.6(3) O(13)–Ni(3)–N(8) 96.3(2) O(11)–Ni(3)–N(8) 91.6(2)
N(7)–Ni(3)–O(15) 94.9(3) O(13)–Ni(3)–O(15) 89.3(2) O(11)–Ni(3)–O(15) 89.1(2)
N(8)–Ni(3)–O(15) 91.6(3) N(7)–Ni(3)–N(9) 95.4(3) O(13)–Ni(3)–N(9) 91.4(2)
O(11)–Ni(3)–N(9) 91.6(2) N(8)–Ni(3)–N(9) 78.1(3) O(15)–Ni(3)–N(9) 169.6(3)