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Fig. 1. Characterization of bulk, 5 h, 10 h and 15 h milled TiO2 nanoparticles prepared by the HEBM method. FESEM images of (A) bulk, (B) 5 h nano TiO2 (C) 10 h nano TiO2 (D) 15 h nanoTiO2. (E) XRD spectra of nanoparticles.