Fig. 3. Sampling experiment.
Reaction conditions: C anode, Pt cathode, constant current = 12 mA, 1a (0.5 mmol), 2a (1.0 mmol), 3a (0.7 ml), nBu4NBF4 (3.0 mmol), MeCN (10 ml), 40°C, GC yields.
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