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. 2018 Jul 7;16(7):230. doi: 10.3390/md16070230

Table 2.

13C-NMR data for 3, 4, 6, and 7 in CD3OD (δ in ppm).

No. 3 a 4 b 6 a 7 a
1 171.0 CO 170.6 CO 173.4 C 173.8 C
3 104.6 CH 98.3 CH 70.6 CH2 70.8 CH2
3a 143.4 C 142.8 C 146.2 C 146.6 C
4 120.5 C 119.9 C 117.6 C 117.9 C
5 165.2 C 164.4 C 164.4 C 164.8 C
6 126.1 C 124.7 C 123.2 C 123.7 C
7 154.6 C 153.6 C 154.2 C 154.7 C
7a 108.7 C 107.1 C 107.3 C 107.7 C
8 11.1 CH3 11.4 CH3 11.4 CH3 11.4 CH3
3-OMe 56.4 CH3 - - -
5-OMe 61.6 CH3 61.2 CH3 61.5 CH3 61.5 CH3
1′ 23.8 CH2 22.9 CH2 23.4 CH2 23.6 CH2
2′ 123.9 CH 122.6 CH 124.2 CH 124.5 CH
3′ 135.4 C 134.6 C 134.7 C 135.1 C
4′ 36.0 CH2 34.8 CH2 35.4 CH2 36.6 CH2
5′ 34.3 CH2 33.1 CH2 33.6 CH2 35.8 CH2
6′ 178.0 C 174.1 C 174.8 C 175.8 C
7′ 16.3 CH3 16.4 CH3 16.2 CH3 16.3 CH3
8′ - - 66.3 CH2 -
9′ - - 70.9 CH -
10′ - - 63.9 CH2 -
6′-OMe - 51.8 CH3 - -
2″ - - - 39.8 CH2
3″ - - - 25.9 CH2
4″ - - - 32.5 CH2
5″ - - - 177.2 C

a Recorded at 100 MHz; b Recorded at 150 MHz.