Table 2.
No. | 3 a | 4 b | 6 a | 7 a |
---|---|---|---|---|
1 | 171.0 CO | 170.6 CO | 173.4 C | 173.8 C |
3 | 104.6 CH | 98.3 CH | 70.6 CH2 | 70.8 CH2 |
3a | 143.4 C | 142.8 C | 146.2 C | 146.6 C |
4 | 120.5 C | 119.9 C | 117.6 C | 117.9 C |
5 | 165.2 C | 164.4 C | 164.4 C | 164.8 C |
6 | 126.1 C | 124.7 C | 123.2 C | 123.7 C |
7 | 154.6 C | 153.6 C | 154.2 C | 154.7 C |
7a | 108.7 C | 107.1 C | 107.3 C | 107.7 C |
8 | 11.1 CH3 | 11.4 CH3 | 11.4 CH3 | 11.4 CH3 |
3-OMe | 56.4 CH3 | - | - | - |
5-OMe | 61.6 CH3 | 61.2 CH3 | 61.5 CH3 | 61.5 CH3 |
1′ | 23.8 CH2 | 22.9 CH2 | 23.4 CH2 | 23.6 CH2 |
2′ | 123.9 CH | 122.6 CH | 124.2 CH | 124.5 CH |
3′ | 135.4 C | 134.6 C | 134.7 C | 135.1 C |
4′ | 36.0 CH2 | 34.8 CH2 | 35.4 CH2 | 36.6 CH2 |
5′ | 34.3 CH2 | 33.1 CH2 | 33.6 CH2 | 35.8 CH2 |
6′ | 178.0 C | 174.1 C | 174.8 C | 175.8 C |
7′ | 16.3 CH3 | 16.4 CH3 | 16.2 CH3 | 16.3 CH3 |
8′ | - | - | 66.3 CH2 | - |
9′ | - | - | 70.9 CH | - |
10′ | - | - | 63.9 CH2 | - |
6′-OMe | - | 51.8 CH3 | - | - |
2″ | - | - | - | 39.8 CH2 |
3″ | - | - | - | 25.9 CH2 |
4″ | - | - | - | 32.5 CH2 |
5″ | - | - | - | 177.2 C |
a Recorded at 100 MHz; b Recorded at 150 MHz.