Table 3.
Gradient program for LC.
| Time (min) | Solvent A (%) | Solvent B (%) |
|---|---|---|
| 0 | 98 | 2 |
| 1.0 | 98 | 2 |
| 8.0 | 0 | 100 |
| 12.0 | 0 | 100 |
| 12.1 | 98 | 2 |
| 14.0 | 98 | 2 |
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