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. 2018 Jul 24;14:1890–1900. doi: 10.3762/bjoc.14.163

Table 2.

ESIMS data of peptide labeling with ligand 3 (cf. Supporting Information File 1 for all details).

Peptide Peptide mass (M) Detected masses after labeling (m/z)

ILMEHIHKL (M2) 1132.6499 531.1584 [M + H]+ a, 832.4043 [M + 2H]2+ b (Figure 5)
YLLPAIVHI (M3) 1037.6274 531.1584 [M + H]+ a, 784.8971 [M + 2H]2+ b (Figure S11, Supporting Information File 1)
EIAMATVTALR (M7) 1174.6380 531.1586 [M + H]+ a, 853.4019 [M + 2H]2+ b (Figure S14, Supporting Information File 1)
ETIGEILKK (M8) 1029.6071 531.1587 [M + H]+ a, 780.8868 [M + 2H]2+ b (Figure S17, Supporting Information File 1)
EGHIARNCRA (T3) 1125.5462 531.1588 [M + H]+ a, no adduct observed (Figure S20, Supporting Information File 1)
RPQYAEASWNAR (S17) 1447.6957 531.1585 [M + H]+ a, 989.9307 [M + 2H]2+ b (Figure S21, Supporting Information File 1)

aInsertion product of 3 − N2 + H2O; bAdduct of 3 − N2 + H2O to the peptide.