Table 1. Crystallographic data for Re–L and Cu–L.
| Crystal data | ||
| CCDC deposition number | CCDC 1821097 | CCDC 1821098 |
| Chemical formula | C15H14N3O6ReS2 | C24H28Cl2CuN4S4 |
| M r | 582.62 | 635.23 |
| Crystal system | Monoclinic | Monoclinic |
| Space group | P21/c | P21/c |
| Temperature (K) | 295 | 295 |
| a (Å) | 26.3056(13) | 19.911(11) |
| b (Å) | 9.4798(4) | 8.771(4) |
| c (Å) | 16.1346(6) | 8.088(4) |
| β (°) | 106.786(2) | 93.416(15) |
| V (Å3) | 3852.1(3) | 1409.9(12) |
| Z | 8 | 2 |
| Radiation type | Mo Kα | Mo Kα |
| μ (mm–1) | 6.56 | 1.28 |
| Crystal size (mm) | 0.43 × 0.19 × 0.16 | 0.17 × 0.16 × 0.06 |
| Absorption correction | Numerical | Numerical |
| T min, Tmax | 0.29, 0.35 | 0.81, 0.93 |
| Reflections | ||
| Measured | 38 228 | 23 119 |
| Independent | 9952 | 2636 |
| Observed [I > 2.0σ(I)] | 6648 | 1881 |
| R int | 0.021 | 0.034 |
| (sin θ/λ)max (Å–1) | 0.682 | 0.613 |
| Refinement | ||
| R[F2 > 2σ(F2)] | 0.036 | 0.047 |
| wR(F2) | 0.054 | 0.101 |
| S | 1.00 | 1.00 |
| No. of reflections | 6648 | 1881 |
| No. of parameters | 487 | 160 |
| H-Atom treatment | H-Atom parameters constrained | H-Atom parameters constrained |
| Δρmax, Δρmin (e Å–3) | 1.68, –2.74 | 0.65, –0.57 |