Table 2. Selected bond lengths [Å] and angles [°] for Re–L.
Distances | |||
Re1–N1 | 2.204(5) | C1–C6 | 1.390(9) |
Re1–N2 | 2.206(5) | C2–C3 | 1.386(9) |
Re1–S1 | 2.4627(16) | C3–C4 | 1.361(11) |
Re1–C13 | 1.889(6) | C4–C5 | 1.407(11) |
Re1–C14 | 1.940(7) | C5–C6 | 1.369(8) |
Re1–C15 | 1.874(6) | C6–C7 | 1.468(8) |
N1–C12 | 1.488(7) | C8–C9 | 1.410(9) |
N2–C7 | 1.300(8) | C8–C10 | 1.445(8) |
N2–C8 | 1.370(7) | C11–C12 | 1.517(8) |
S1–C10 | 1.778(6) | C13–O1 | 1.171(7) |
S1–C11 | 1.830(6) | C14–O2 | 1.135(7) |
S2–C7 | 1.737(6) | C15–O3 | 1.170(7) |
S2–C9 | 1.654(8) |
Angles | |||
N1–Re1–N2 | 84.33(18) | S1–Re1–C14 | 177.13(19) |
N1–Re1–S1 | 80.56(13) | C13–Re1–C14 | 89.5(3) |
N2–Re1–S1 | 79.57(13) | N1–Re1–C15 | 91.6(2) |
N1–Re1–C13 | 173.8(2) | N2–Re1–C15 | 173.6(2) |
N2–Re1–C13 | 93.4(2) | S1–Re1–C15 | 94.9(2) |
S1–Re1–C13 | 93.40(19) | C13–Re1–C15 | 90.1(3) |
N1–Re1–C14 | 96.6(2) | C14–Re1–C15 | 85.4(3) |
N2–Re1–C14 | 99.9(2) | C14–Re1–C15 | 85.4(3) |