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. 2018 Jul 10;74(Pt 8):1071–1074. doi: 10.1107/S2056989018009544

Table 3. Experimental details.

Crystal data
Chemical formula C15H14N2O2
M r 254.28
Crystal system, space group Orthorhombic, P212121
Temperature (K) 296
a, b, c (Å) 7.6419 (7), 11.8889 (13), 14.8082 (16)
V3) 1345.4 (2)
Z 4
Radiation type Mo Kα
μ (mm−1) 0.09
Crystal size (mm) 0.15 × 0.10 × 0.10
 
Data collection
Diffractometer Bruker APEXII CCD
Absorption correction Multi-scan (SADABS; Bruker, 2012)
T min, T max 0.841, 0.992
No. of measured, independent and observed [I > 2σ(I)] reflections 20309, 2535, 1401
R int 0.055
(sin θ/λ)max−1) 0.612
 
Refinement
R[F 2 > 2σ(F 2)], wR(F 2), S 0.040, 0.120, 1.04
No. of reflections 2535
No. of parameters 209
No. of restraints 17
H-atom treatment H-atom parameters constrained
Δρmax, Δρmin (e Å−3) 0.11, −0.11

Computer programs: APEX2 and SAINT (Bruker, 2012), SHELXS97 (Sheldrick, 2008), SHELXL2014 (Sheldrick, 2015) and PLATON (Spek, 2009).