Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C9H10N5 +·C7H7O3S− |
| M r | 359.41 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 296 |
| a, b, c (Å) | 11.0060 (6), 20.7269 (11), 7.6213 (4) |
| β (°) | 97.468 (2) |
| V (Å3) | 1723.83 (16) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.21 |
| Crystal size (mm) | 0.35 × 0.35 × 0.30 |
| Data collection | |
| Diffractometer | Bruker Kappa APEXII CCD |
| Absorption correction | Multi-scan (SADABS; Bruker, 2004 ▸) |
| T min, T max | 0.929, 0.939 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 20842, 4273, 3325 |
| R int | 0.033 |
| (sin θ/λ)max (Å−1) | 0.667 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.049, 0.151, 1.01 |
| No. of reflections | 4277 |
| No. of parameters | 227 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.49, −0.43 |