Bruker SMART APEXII diffractometer | 2612 independent reflections |
Radiation source: fine-focus sealed tube | 2503 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.015 |
ω scans | θmax = 29.0°, θmin = 2.6° |
Absorption correction: multi-scan (SADABS; Bruker, 2008) | h = −8→8 |
Tmin = 0.917, Tmax = 0.995 | k = −7→5 |
4329 measured reflections | l = −21→20 |