Bruker SMART APEXII diffractometer | 2455 independent reflections |
Radiation source: fine-focus sealed tube | 1914 reflections with I > 2σ(I) |
Graphite monochromator | Rint = 0.030 |
ω scans | θmax = 29.0°, θmin = 2.9° |
Absorption correction: multi-scan (SADABS; Bruker, 2008) | h = −8→8 |
Tmin = 0.827, Tmax = 0.996 | k = −7→7 |
4142 measured reflections | l = −14→19 |