Table 2. Experimental details.
| Crystal data | |
| Chemical formula | C13H6Cl3FOS |
| M r | 335.60 |
| Crystal system, space group | Monoclinic, P21/c |
| Temperature (K) | 294 |
| a, b, c (Å) | 3.9564 (8), 13.367 (2), 25.173 (5) |
| β (°) | 93.363 (4) |
| V (Å3) | 1329.0 (4) |
| Z | 4 |
| Radiation type | Mo Kα |
| μ (mm−1) | 0.84 |
| Crystal size (mm) | 0.44 × 0.19 × 0.14 |
| Data collection | |
| Diffractometer | Bruker APEXII DUO CCD area-detector |
| Absorption correction | Multi-scan (SADABS; Bruker, 2012 ▸) |
| T min, T max | 0.708, 0.894 |
| No. of measured, independent and observed [I > 2σ(I)] reflections | 3901, 3901, 2430 |
| R int | 0.000 |
| (sin θ/λ)max (Å−1) | 0.707 |
| Refinement | |
| R[F 2 > 2σ(F 2)], wR(F 2), S | 0.076, 0.218, 1.04 |
| No. of reflections | 3901 |
| No. of parameters | 173 |
| H-atom treatment | H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) | 0.46, −0.48 |