| Rigaku Oxford Diffraction diffractometer | 12901 independent reflections |
| Radiation source: Enhance (Mo) X-ray Source | 9324 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.029 |
| Detector resolution: 16.0416 pixels mm-1 | θmax = 32.8°, θmin = 3.1° |
| ω scans | h = −16→16 |
| Absorption correction: multi-scan (CrysAlis PRO; Agilent, 2014) | k = −17→17 |
| Tmin = 0.836, Tmax = 1.000 | l = −23→23 |
| 24707 measured reflections |
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