| Crystal data |
| Chemical formula |
[Mn(C2H3O2)(C18H18N4)(CH4O)](C24H20B) |
|
M
r
|
755.60 |
| Crystal system, space group |
Triclinic, P
|
| Temperature (K) |
173 |
|
a, b, c (Å) |
11.3885 (8), 11.7598 (7), 15.6703 (10) |
| α, β, γ (°) |
82.041 (5), 70.671 (6), 85.870 (5) |
|
V (Å3) |
1960.5 (2) |
|
Z
|
2 |
| Radiation type |
Mo Kα |
| μ (mm−1) |
0.38 |
| Crystal size (mm) |
0.44 × 0.38 × 0.26 |
| |
| Data collection |
| Diffractometer |
Rigaku Oxford Diffraction |
| Absorption correction |
Multi-scan (CrysAlis PRO; Agilent, 2014 ▸) |
|
T
min, T
max
|
0.836, 1.000 |
| No. of measured, independent and observed [I > 2σ(I)] reflections |
24707, 12901, 9324 |
|
R
int
|
0.029 |
| (sin θ/λ)max (Å−1) |
0.763 |
| |
| Refinement |
|
R[F
2 > 2σ(F
2)], wR(F
2), S
|
0.047, 0.122, 1.03 |
| No. of reflections |
12901 |
| No. of parameters |
492 |
| No. of restraints |
3 |
| H-atom treatment |
H-atom parameters constrained |
| Δρmax, Δρmin (e Å−3) |
0.36, −0.30 |
