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Rietveld refinement data for Ni2B and Ni3B from Run 5 and Run 9.
| Formula | Ni3B (This Work) |
Ni3B [6] | Ni2B (This Work) |
Ni2B [32] |
|---|---|---|---|---|
| Crystal System | Orthorhombic (Pnma) | Tetragonal (I4/mcm) | ||
| a(Å) | 5.2273 (1) | 5.2195 (5) | 4.9768 (1) | 4.9910 (3) |
| b(Å) | 6.6131 (1) | 6.6164 (6) | 4.9768 (1) | 4.9910 (3) |
| c(Å) | 4.3900 (1) | 4.3912 (4) | 4.2348 (0) | 4.2470 (3) |
| Cell Vol. (Å3) | 151.756 (3) | 151.65 | 104.891 (2) | 105.79 |
| Rwp | 5.4 | 3.86 | ||
| Rp | 3.86 | 2.61 | ||
| GoF | 2.57 | 1.81 | ||
