Table 2.
1H NMR peak assignment of sugarcane bagasse lignin extracted with [EMIM]oAc
| Signal (ppm) | Functional group |
|---|---|
| 1–1.5 | Proton in aliphatic acetate |
| 0.7–0.9 | Aliphatic contaminants |
| 2.2–2.6 | Proton in aromatic acetate |
| 3.2–3.4 | Hβ in β–β structure |
| 3.4–4 | Methoxyl proton |
| 4.1–4.6 | Hγ in β-O-4 aryl ether |
| 4.8 | Hβ in β-O-4 aryl ether |
| 5.3–5.8 | Hβ in benzyl aryl ether |
| 6.6 | Aromatic H in syringyl unit |
| 6.7–6.9 | Aromatic H in guaiacyl unit |
| 7.3–7.6 | Ethylenic and aromatic protons in p-coumaric and ferulic acids |