Table 2.
Analytical Methodb | Bastille | Dante | Hot Harold | ||||||
---|---|---|---|---|---|---|---|---|---|
Inner | Outer | Bulk Sample | Inner | Outer | Bulk Sample | Inner | Bulk sample | ||
Fe% | INAA | 33.00 | 33.10 | 31.50 | 0.73 | 38.60 | 3.86 | 19.10 | 0.91 |
Cu% | ICP-OES | 10.00 | 2.18 | 4.64 | 0.11 | 0.48 | 1.18 | 0.33 | 0.09 |
Zn% | ICP-OES | 2.03 | 6.31 | 3.33 | 0.68 | 0.44 | 0.20 | 0.83 | 1.29 |
S% | IR (Leco) | 40.2 | 43.4 | 40.2 | 25.7 | 40.5 | 27.4 | 34.1 | 25.6 |
SiO2% | ICP-OES | 4.62 | 6.93 | 3.29 | 0.24 | 0.26 | 0.19 | <0.02 | 0.90 |
Ba% | INAA | 0.48 | 0.42 | 0.40 | 0.09 | 0.01 | 0.03 | 0.04 | 0.07 |
Al2O3% | ICP-OES | 1.47 | 0.34 | 0.45 | 0.02 | 0.06 | 0.02 | <0.02 | 0.02 |
Pb% | ICP-MS | 0.03 | 0.06 | 0.04 | 0.01 | 0.03 | 0.00 | 0.02 | 0.01 |
CaO% | ICP-OES | 0.10 | <0.01 | 4.88 | 39.46 | 7.82 | 37.22 | 24.91 | 38.90 |
MgO% | ICP-OES | 0.05 | <0.02 | 0.02 | 0.15 | 0.18 | 0.07 | <0.02 | 0.5 |
Na2O% | ICP-OES | 0.53 | 0.08 | 0.22 | 0.67 | 0.89 | 0.27 | 0.47 | 0.54 |
Totalc | 92.5 | 92.8 | 89.0 | 67.9 | 89.3 | 70.4 | 79.8 | 68.8 |
aThe results are reported in concentrations of elemental and oxide weight percent (wt %).
bINAA, Instrumental Neutron Activation Analysis; ICP-OES, Inductively Coupled Plasma-Optical Emission Spectroscopy; IR, Infrared Detection; ICP-MS, Inductively Coupled Plasma-Mass Spectrometry.
cLow totals are largely attributed to the exclusion of sulfate-bonded oxygen in the analyses.