Table 1.
Position | 1H * | 13C * |
---|---|---|
1 | - | 133.9 |
2 | - | 160.6 |
3 | - | 105.2 |
4 | - | 162.6 |
5 | 6.65 (d, 8.1) | 115.5 |
6 | 7.47 (d, 8.1) | 132.5 |
1′ | 4.84 ** | 77.3 |
2′ | 3.70 (m) | 74.3 |
3′ | 3.38 (m) | 80.0 |
4′ | 3.38 (m) | 71.0 |
5′ | 3.30 (m) | 82.5 |
6′ | 3.68 (m) | 62.1 |
Carbonyl | - | 198.6 |
* Solvent signal as reference. ** Overlapped with signal of residual water.