Table 1.
RT | RIC | RIL | Compounds | PEE % | DCME % | EO * % | Identification |
---|---|---|---|---|---|---|---|
20.16 | 1327 | 1343 | α-cubebene | 0.09 | - | 0.05 | RI, MS |
20.82 | 1353 | 1359 | copaene | 0.75 | 0.55 | 0.71 | RI, MS |
21.13 | 1364 | 1387 | β-cubebene | 0.07 | - | - | RI, MS |
22.66 | 1424 | 1428 | α-caryophyllene | 0.08 | 0.15 | 1.27 | RI, MS |
23.13 | 1443 | 1445 | bicyclosesquiphellandrene | - | 0.46 | - | RI, MS |
23.2 | 1446 | 1462 | γ-muurolene | 0.33 | - | - | RI, MS |
23.77 | 1468 | 1469 | α-muurolene | 0.85 | 0.63 | - | RI, MS |
24.17 | 1484 | 1509 | (−)-trans-calamenene | 7.06 | 5.26 | - | RI, MS,NMR |
24.28 | 1488 | 1515 | δ-cadinene | 2.75 | 6.43 | 10.8 | RI, MS |
24.5 | 1497 | 1524 | 4,5,9,10-dehydroisolongifolene | 0.27 | 2.14 | - | RI, MS |
24.6 | 1501 | 1522 | α-calacorene | 0.72 | 5.12 | 0.95 | RI, MS |
25.5 | 1540 | 1549 | caryophyllene oxide | 3.12 | 0.48 | 1.02 | RI, MS |
25.67 | 1547 | 1553 | germacrene B | 3.00 | 2.6 | - | RI, MS |
26.08 | 1565 | 1588 | 1,2-epoxyhumulene | 2.06 | 0.34 | 0.51 | RI, MS |
26.65 | 1588 | 1620 | (−)-torreyol | 18.1 | 18.53 | 24.16 | RI, MS,NMR |
26.98 | 1602 | 1627 | (−)-epi-cubenol | 10.14 | 8.01 | 12.44 | RI, MS,NMR |
26.98 | 1602 | 1628 | (−)-cubenol | 7.0 | 8.1 | 10.5 | RI, MS,NMR |
27.17 | 1611 | - | (−)-15-copaenol | 14.25 | 12.5 | 15.46 | MS,NMR |
27.33 | 1618 | - | cadala-1(10),3,8-triene | 2.03 | 1.57 | - | MS |
27.52 | 1627 | 1652 | cadalene | 0.86 | 3.66 | - | RI, MS,NMR |
35.04 | 1991 | - | 7-isopropyl-1,1,4a-trimethyl-1,2,3,4,4a,9,10,10a-octahydrophenanthrene | 0.19 | - | - | MS |
39.55 | 2243 | - | 6,7-dehydroferruginol | 3.76 | 1.06 | - | MS |
39.63 | 2248 | - | ferruginol | 4.28 | 1.13 | - | MS |
42.92 | 2450 | - | hinokione | 0.26 | 0.25 | - | MS |
43.53 | 2489 | - | hinokiol | 0.29 | 0.75 | - | MS |
44.14 | 2529 | - | sugiol | 0.12 | 0.12 | - | MS |