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. 2018 May 25;23(6):1263. doi: 10.3390/molecules23061263

Table 1.

NMR data for 1 and 2.

Pos. 1 2
δCa, Mult. δHb (J in Hz) HMBC δCc Mult. δHd (J in Hz) HMBC
1 134.0, qC 126.6, qC
2 112.8, CH 6.90, s 1, 3, 4, 4a, 10b 112.8, CH 6.93, s 1, 3, 4, 10a, 10b, 12
3 153.8, qC 147.8, qC
4 128.0, qC 140.6, qC
4a 147.0, qC 138.8, qC
6 164.4, qC 164.8, qC
6a 98.9, qC 98.2, qC
7 165.0, qC 165.0, qC
8 99.5, CH 6.60, d (2.0) 7, 6a, 10a 101.3, CH 6.46, d (2.0) 6a, 9, 10
9 166.7, qC 165.3, qC
10 104.2, CH 7.28, d (2.0) 6a, 9, 10a 104.9, CH 7.37, d (2.0) 6a, 8, 9, 10b
10a 137.9, qC 132.8, qC
10b 111.0, qC 111.2, qC
11 55.4, CH3 3.96, s 9 55.7, CH3 3.67, s 3
12 55.2, CH3 3.67, s 3 24.5, CH3 2.75, s 1, 2, 10, 10a
13 24.8, CH3 2.78, s 1, 2
1′ 105.4, qC
2′ 195.9, qC
2′a 117.4, qC
3′ 139.8, qC
4′ 123.8, CH 6.88, d (7.8) 5′, 6′, 7′
5′ 137.7, CH 7.45, t (7.8) 4′, 6′a
6′ 109.8, CH 6.72, d (7.8) 2′a, 5′
6′a 170.0, qC
7′ 16.7, CH3 2.53, s 2′a, 3′, 4′
8′ 19.4, CH3 1.80, s 1′, 2′
OH-7 11.89, s 7, 8 11.95, s 6a, 7, 8

a Recorded at 100 MHz in acetone-d6; b Recorded at 400 MHz in acetone-d6; c Recorded at 150 MHz in acetone-d6; d Recorded at 600 MHz in acetone-d6.