Table 3.
Analytes | Sample (g) | Origin (μg) | Spiked (μg) | Found (μg) | Mean Recovery (%) (RSD, %) |
---|---|---|---|---|---|
Monotropein | 0.5 | 1848.45 | 1480 | 3304.33 | 98.37 (3.23) |
1850 | 3680.69 | 99.04 (2.15) | |||
2220 | 4059.13 | 99.58 (3.06) | |||
Deacetyl asperulosidic acid | 0.5 | 1883.74 | 1500 | 3351.19 | 97.83 (4.07) |
1880 | 3731.03 | 98.26 (2.38) | |||
2260 | 4113.01 | 98.64 (1.95) | |||
Asperulosidic acid | 0.5 | 174.43 | 140 | 310.70 | 97.33 (2.84) |
175 | 346.00 | 98.04 (3.37) | |||
210 | 384.14 | 99.86 (3.69) | |||
Asperuloside | 0.5 | 56.32 | 45 | 100.61 | 98.41 (4.23) |
55 | 110.13 | 97.83 (3.94) | |||
67.5 | 122.63 | 98.23 (2.78) | |||
Rubiadin-1-methyl ether | 0.5 | 69.53 | 55 | 122.58 | 96.47 (2.94) |
70 | 136.56 | 95.77 (2.62) | |||
84 | 149.59 | 95.32 (3.15) | |||
Rubiadin | 0.5 | 17.62 | 14 | 31.27 | 97.48 (1.75) |
17.5 | 34.63 | 97.17 (2.77) | |||
21 | 37.88 | 96.48 (3.28) |