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. 2018 Apr 25;23(5):1007. doi: 10.3390/molecules23051007

Table 2.

Polymerization reactions of aL-9-ΝΒΕ with different concentrations of GC-I catalyst 1.

Entry GC-I (mg, [mmol]) [GC-I] (% w/w, [mM]) GC-I/Monomer (mol/mol) Apparent Gelation Time 2 (min)
1 20 [0.024] 0.20 [2.4] 1/25 15
2 10 [0.012] 0.10 [1.2] 1/50 60
3 5 [0.006] 0.05 [0.6] 1/100 140
4 1 [0.0012] 0.01 [0.12] 1/500 -

1 aL-9-NBE: 1.2 g, 0.6 mmol, 12.2% w/w; solvent: toluene (10 mL); 2 Until the sol stopped flowing.