Table 4.
Average recoveries (%), intra-day repeatability (%RSD), and limits of detection (LOD, (µg/dm3) and quantification (LOQ, (µg/dm3)) obtained with the optimized method in spiked chicken meat samples, analyzed using GC–MS (n = 4 at each level)
| Analyte | Concentration level 0.15 mg/dm3 |
LOD/µg/dm3 | LOQ/µg/dm3 | |
|---|---|---|---|---|
| Recovery/% | Intra-day/%RSD | |||
| CAD | 82 | 4 | 1.5 | 4.5 |
| HIST | 74 | 4 | 4.2 | 12.6 |
| PUT | 88 | 2 | 1.4 | 4.6 |
| TYR | 89 | 3 | 3.3 | 9.9 |