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. Author manuscript; available in PMC: 2019 Sep 15.
Published in final edited form as: J Chromatogr B Analyt Technol Biomed Life Sci. 2018 Jul 20;1095:112–118. doi: 10.1016/j.jchromb.2018.07.017

Table 3.

Stability of QCs and calibrators during ten freeze-thaw cycles and storage at temperatures of 4, 22, and 60 °C for up to 24 hours (n=3).

HGA (%Recovery)* MCPG (%Recovery)*

QH QM QL QH QM QL
4 °C 101 89.6 96.5 107 90.8 97.3
22 °C 94.2 102 86.1 106 104 98.8
Freeze Thaw 105 128 122 109 134 121

S8 S5 S2 S8 S5 S2

60 °C 92.6 95.6 99.9 95.4 98.4 105
*

%Recovery, ( %Recovery=Conc2Conc1×100%)