. 2018 Jul 11;9(32):6639–6646. doi: 10.1039/c8sc02253d

Table 1. Initial reaction screening ^a .


Entry	Conditions	Yield 1 ^b	Yield 2 ^b	Yield 3 ^b
1	As shown	0%	0%	35%
2	No light	100%	100%	0%
3	No silane	100%	100%	0%
4	No [Ir] cat.	100%	100%	0%
5	No base	8%	21%	30%

^a N-Phenylmetacrylamide (1) (1.0 equiv.), (4-bromopiperidin-1-yl)(phenyl)methanone (2) (1.0 equiv.), Na₂CO₃ (2.0 equiv.), (Me₃Si)₃SiH (1.0 equiv.) and Ir[dF(CF₃)ppy]₂(dtbbpy)PF₆ (1 mol%) in MeCN, Aldrich® Micro Photochemical Reactor (ring) for 16 h.

^bAssay yields for product and remaining starting materials were determined using HPLC techniques.

Table 1. Initial reaction screening a .

Table 1. Initial reaction screening ^a .