Table 3.
Pos. | 3 (in CDCl3) | 4 (in CDCl3) | 5 (in CDCl3) | 6 (in CD3OD) | 7 (in CD3OD) | 8 (in CD3OD) |
---|---|---|---|---|---|---|
1 | 68.6, C | 68.7, C | 209.7, C | 200.1, C | 171.1, C | |
2 | 39.8, CH2 | 39.8, CH2 | 35.4, CH2 | 44.0, CH2 | 153.4, CH | |
3 | 121.8, CH | 122.0, CH | 27.9, CH2 | 68.4, CH | 88.5, CH | |
4 | 135.6, C | 135.6, C | 184.4, C | 175.4, C | 31.8, CH2 | 140.1, C |
5 | 24.3, CH2 | 24.1, CH2 | 128.1, CH | 131.5, C | 25.3, CH2 | 136.5, CH |
6 | 35.4, CH2 | 35.4, CH2 | 68.0, CH | 66.3, CH | 60.5, CH | 22.4, CH2 |
7 | 46.3, CH | 46.3, CH | 22.2, CH3 | 21.8, CH3 | 173.6, C | 33.7, CH2 |
8 | 15.6, CH3 | 15.7, CH3 | 176.2, C | |||
9 | 179.5, C | 179.7, C | 55.0, CH | |||
10 | 28.6, CH3 | 28.4, CH3 | 38.8, CH2 | |||
11 | 25.9, CH | |||||
12 | 23.4, CH3 | |||||
13 | 22.0, CH3 | |||||
14 | 57.4, CH3 |