Table 4.
Zebrafish TRAP1 bound to AMPPNP and calcium | |
---|---|
Wavelength | 1.116 |
Resolution range | 48.4–2.5 (2.591–2.5) |
Space group | C 1 2 1 |
Unit cell | 176.252 95.751 124.546 90 134.663 90 |
Unique reflections | 49,471 (4,870) |
Completeness (%) | 97.6 |
Mean I/σ(I) | 10.36 |
Wilson B-factor | 61.0 |
Rmeas | 11.3% |
CC1/2 | 99.6% |
Reflections used in refinement | 47,254 (4,868) |
Reflections used for Rfree | 2,488 (251) |
Rwork | 0.230 (0.4170) |
Rfree | 0.253 (0.4471) |
Number of non-hydrogen atoms | 9,794 |
Macromolecules | 9,553 |
Ligands | 64 |
Solvent | 177 |
Protein residues | 1,185 |
Root mean square (bonds) | 0.016 |
Root mean square (angles) | 1.31 |
Ramachandran favored (%) | 93.67 |
Ramachandran allowed (%) | 5.12 |
Ramachandran outliers (%) | 1.21 |
Rotamer outliers (%) | 9.65 |
Clashscore | 11.10 |
Average B-factor | 73.67 |
Macromolecules | 74.35 |
Ligands | 42.12 |
Solvent | 48.43 |
Number of TLS groups | 7 |