Table 1.
Table of 13C NMR Spectroscopic data of 10 flavonoid compounds in DMSO-d6.
GF-1 | GF-2 | GF-3 | GF-4 | GF-5 | GF-6 | GF-7 | GF-8 | GF-9 | GF-10 | |
---|---|---|---|---|---|---|---|---|---|---|
C-1 | 113.5 | 125.7 | ||||||||
C-2 | 155.7 | 155.1 | 162.5 | 157.9 | 153.0 | 158.2 | 78.9 | 131.1 | 162.2 | 155.8 |
C-3 | 120.5 | 122.1 | 104.4 | 102.7 | 124.2 | 99.9 | 43.1 | 115.8 | 104.4 | 137.7 |
C-4 | 180.6 | 176.0 | 176.2 | 158.6 | 174.5 | 159.6 | 190.0 | 160.3 | 176.2 | 178.0 |
C-4a | 104.6 | 116.2 | 16.1 | 100.2 | 127.2 | 113.5 | 115.8 | 105.1 | ||
C-5 | 161.8 | 127.2 | 126.4 | 154.3 | 116.6 | 126.5 | 128.3 | 115.8 | 124.5 | 160.9 |
C-6 | 98.8 | 115.3 | 114.7 | 120.1 | 115.0 | 127.7 | 110.5 | 131.1 | 127.2 | 97.6 |
C-7 | 164.1 | 162.8 | 160.6 | 160.0 | 162.5 | 164.6 | 160.3 | 165.0 | ||
C-8 | 93.6 | 102.0 | 102.4 | 99.7 | 102.0 | 102.5 | 101.7 | 92.2 | ||
C-8a | 157.7 | 157.5 | 157.3 | 153.4 | 158.9 | 163.1 | 155.6 | 160.2 | ||
C-α | 117.8 | 144.2 | ||||||||
C-β | 138.7 | 117.4 | ||||||||
C-γ | 187.3 | 191.5 | ||||||||
C-1′ | 111.2 | 112.7 | 121.7 | 114.7 | 123.1 | 129.6 | 129.3 | 112.9 | 121.9 | 120.4 |
C-2′ | 151.2 | 151.3 | 128.0 | 156.6 | 130.0 | 130.6 | 128.2 | 165.8 | 127.9 | 130.1 |
C-3′ | 109.7 | 110.1 | 115.8 | 99.0 | 113.5 | 115.2 | 115.1 | 102.5 | 115.8 | 115.6 |
C-4′ | 153.6 | 153.5 | 162.4 | 157.4 | 157.4 | 161.6 | 157.6 | 165.4 | 160.5 | 156.2 |
C-5′ | 107.4 | 107.6 | 115.8 | 114.5 | 113.5 | 115.2 | 115.1 | 108.0 | 115.8 | 115.6 |
C-6′ | 131.3 | 130.9 | 128.0 | 120.9 | 130.0 | 130.6 | 128.2 | 132.7 | 127.9 | 130.1 |
C-1″ | 22.5 | 39.5 | 27.5 | |||||||
C-2″ | 75.4 | 75.4 | 122.9 | 147.5 | 121.8 | |||||
C-3″ | 128.8 | 128.8 | 131.4 | 109.9 | 132.3 | |||||
C-4″ | 116.9 | 117.0 | 18.2 | 26.9 | 25.5 | |||||
C-5″ | 27.4 | 27.5 | 25.9 | 26.9 | 17.6 | |||||
C-6″ | 27.4 | 27.5 | ||||||||
2-OCH3 | 55.4 | |||||||||
3-OCH3 | 56.0 | |||||||||
4′-OCH3 | 55.1 | |||||||||
5-OCH3 | 62.8 | |||||||||
7-OCH3 | 59.6 |