Table 2. Data-collection statistics for subsets of native proteinase K data.
Values in parentheses are for the outer shell.
| 6000 images | 5000 images | 4000 images | 3000 images | |
|---|---|---|---|---|
| Wavelength (Å) | 1.033 | 1.033 | 1.033 | 1.033 |
| Resolution range (Å) | 19.91–2.04 (2.11–2.04) | 19.91–2.04 (2.11–2.04) | 19.91–2.04 (2.11–2.04) | 19.91–2.04 (2.11–2.04) |
| Space group | P43212 | P43212 | P43212 | P43212 |
| a, b, c (Å) | 67.6, 67.6, 107.4 | 67.6, 67.6, 107.4 | 67.6, 67.6, 107.4 | 67.6, 67.6, 107.46 |
| α, β, γ (°) | 90.0, 90.0, 90.0 | 90.0, 90.0, 90.0 | 90.0, 90.0, 90.0 | 90.0, 90.0, 90.0 |
| Total reflections | 1605620 (25039) | 1339372 (21218) | 1065881 (18213) | 801425 (14459) |
| Unique reflections | 32117 (3211) | 32117 (3211) | 32117 (3211) | 32117 (3211) |
| Multiplicity | 50.0 (7.9) | 41.8 (6.7) | 33.3 (5.9) | 25.2 (4.9) |
| Completeness (%) | 99.93 (99.28) | 99.81 (98.16) | 99.67 (96.95) | 99.20 (92.84) |
| Mean I/σ(I) | 5.35 (2.81) | 4.96 (3.23) | 4.49 (3.09) | 4.03 (3.57) |
| R split (%) | 17.14 (41.84) | 18.73 (44.41) | 20.93 (46.02) | 24.30 (49.58) |
| CC* | 0.987 (0.903) | 0.985 (0.892) | 0.982 (0.879) | 0.974 (0.868) |
| CCano | 0.03 | 0.03 | 0.02 | 0.02 |