| Rigaku Xcalibur Atlas Gemini ultra diffractometer | 2508 independent reflections |
| Radiation source: fine-focus sealed X-ray tube, Enhance (Mo) X-ray Source | 1563 reflections with I > 2σ(I) |
| Graphite monochromator | Rint = 0.033 |
| Detector resolution: 10.4186 pixels mm-1 | θmax = 29.6°, θmin = 2.8° |
| ω scans | h = −7→7 |
| Absorption correction: multi-scan (CrysAlis PRO; Rigaku OD, 2015) | k = −12→12 |
| Tmin = 0.720, Tmax = 1.000 | l = −13→14 |
| 7946 measured reflections |
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