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. 2018 Aug 31;74(Pt 9):1369–1372. doi: 10.1107/S205698901801201X
Cu1—O1 1.934 (3) C11—H11A 0.9800
Cu1—O1i 1.944 (3) C11—H11B 0.9800
Cu1—Cl1 2.2326 (13) C11—H11C 0.9800
Cu1—Cl2 2.2395 (12) C12—H12A 0.9800
O1—C1 1.398 (4) C12—H12B 0.9800
O1—Cu1i 1.944 (3) C12—H12C 0.9800
N1—C2 1.334 (5) C13—H13A 0.9800
N1—C3 1.386 (6) C13—H13B 0.9800
N1—C5 1.463 (5) C13—H13C 0.9800
N2—C2 1.341 (5) C14—C15 1.381 (7)
N2—C4 1.381 (6) C14—C19 1.410 (7)
N2—C14 1.432 (5) C15—C16 1.404 (7)
C1—C2 1.497 (6) C15—C20 1.511 (7)
C1—H1A 0.9900 C16—C17 1.390 (7)
C1—H1B 0.9900 C16—H16 0.9500
C3—C4 1.345 (6) C17—C18 1.369 (7)
C3—H3 0.9500 C17—C21 1.507 (6)
C4—H4 0.9500 C18—C19 1.383 (6)
C5—C10 1.368 (6) C18—H18 0.9500
C5—C6 1.383 (6) C19—C22 1.502 (6)
C6—C7 1.392 (6) C20—H20A 0.9800
C6—C11 1.488 (7) C20—H20B 0.9800
C7—C8 1.365 (7) C20—H20C 0.9800
C7—H7 0.9500 C21—H21A 0.9800
C8—C9 1.374 (7) C21—H21B 0.9800
C8—C12 1.528 (6) C21—H21C 0.9800
C9—C10 1.398 (6) C22—H22A 0.9800
C9—H9 0.9500 C22—H22B 0.9800
C10—C13 1.513 (7) C22—H22C 0.9800
O1—Cu1—O1i 74.10 (11) C6—C11—H11C 109.5
O1—Cu1—Cl1 162.46 (10) H11A—C11—H11C 109.5
O1i—Cu1—Cl1 95.69 (9) H11B—C11—H11C 109.5
O1—Cu1—Cl2 95.60 (8) C8—C12—H12A 109.5
O1i—Cu1—Cl2 162.36 (9) C8—C12—H12B 109.5
Cl1—Cu1—Cl2 97.58 (5) H12A—C12—H12B 109.5
C1—O1—Cu1 127.2 (3) C8—C12—H12C 109.5
C1—O1—Cu1i 126.8 (3) H12A—C12—H12C 109.5
Cu1—O1—Cu1i 105.90 (11) H12B—C12—H12C 109.5
C2—N1—C3 109.5 (4) C10—C13—H13A 109.5
C2—N1—C5 129.0 (4) C10—C13—H13B 109.5
C3—N1—C5 121.5 (4) H13A—C13—H13B 109.5
C2—N2—C4 109.3 (4) C10—C13—H13C 109.5
C2—N2—C14 127.0 (4) H13A—C13—H13C 109.5
C4—N2—C14 123.6 (3) H13B—C13—H13C 109.5
O1—C1—C2 113.2 (3) C15—C14—C19 123.5 (4)
O1—C1—H1A 108.9 C15—C14—N2 119.0 (5)
C2—C1—H1A 108.9 C19—C14—N2 117.5 (4)
O1—C1—H1B 108.9 C14—C15—C16 116.6 (5)
C2—C1—H1B 108.9 C14—C15—C20 122.3 (5)
H1A—C1—H1B 107.8 C16—C15—C20 121.1 (5)
N1—C2—N2 107.2 (4) C17—C16—C15 121.4 (5)
N1—C2—C1 131.5 (3) C17—C16—H16 119.3
N2—C2—C1 121.3 (4) C15—C16—H16 119.3
C4—C3—N1 106.8 (4) C18—C17—C16 119.6 (5)
C4—C3—H3 126.6 C18—C17—C21 120.9 (5)
N1—C3—H3 126.6 C16—C17—C21 119.4 (5)
C3—C4—N2 107.2 (4) C17—C18—C19 122.0 (5)
C3—C4—H4 126.4 C17—C18—H18 119.0
N2—C4—H4 126.4 C19—C18—H18 119.0
C10—C5—C6 123.5 (4) C18—C19—C14 116.9 (5)
C10—C5—N1 117.6 (4) C18—C19—C22 120.9 (5)
C6—C5—N1 118.5 (4) C14—C19—C22 122.2 (4)
C5—C6—C7 116.8 (5) C15—C20—H20A 109.5
C5—C6—C11 123.9 (4) C15—C20—H20B 109.5
C7—C6—C11 119.3 (5) H20A—C20—H20B 109.5
C8—C7—C6 121.9 (5) C15—C20—H20C 109.5
C8—C7—H7 119.0 H20A—C20—H20C 109.5
C6—C7—H7 119.0 H20B—C20—H20C 109.5
C7—C8—C9 119.1 (4) C17—C21—H21A 109.5
C7—C8—C12 120.0 (5) C17—C21—H21B 109.5
C9—C8—C12 120.9 (6) H21A—C21—H21B 109.5
C8—C9—C10 121.6 (5) C17—C21—H21C 109.5
C8—C9—H9 119.2 H21A—C21—H21C 109.5
C10—C9—H9 119.2 H21B—C21—H21C 109.5
C5—C10—C9 117.0 (5) C19—C22—H22A 109.5
C5—C10—C13 122.1 (4) C19—C22—H22B 109.5
C9—C10—C13 120.9 (5) H22A—C22—H22B 109.5
C6—C11—H11A 109.5 C19—C22—H22C 109.5
C6—C11—H11B 109.5 H22A—C22—H22C 109.5
H11A—C11—H11B 109.5 H22B—C22—H22C 109.5
Cu1—O1—C1—C2 −95.8 (4) C7—C8—C9—C10 0.1 (9)
Cu1i—O1—C1—C2 87.6 (4) C12—C8—C9—C10 179.5 (6)
C3—N1—C2—N2 0.6 (5) C6—C5—C10—C9 5.5 (7)
C5—N1—C2—N2 −178.9 (4) N1—C5—C10—C9 177.7 (5)
C3—N1—C2—C1 −178.0 (5) C6—C5—C10—C13 −174.4 (5)
C5—N1—C2—C1 2.5 (8) N1—C5—C10—C13 −2.1 (7)
C4—N2—C2—N1 −0.3 (6) C8—C9—C10—C5 −2.9 (8)
C14—N2—C2—N1 176.7 (5) C8—C9—C10—C13 177.0 (5)
C4—N2—C2—C1 178.5 (4) C2—N2—C14—C15 95.2 (6)
C14—N2—C2—C1 −4.5 (7) C4—N2—C14—C15 −88.2 (6)
O1—C1—C2—N1 0.2 (7) C2—N2—C14—C19 −88.1 (5)
O1—C1—C2—N2 −178.3 (4) C4—N2—C14—C19 88.6 (6)
C2—N1—C3—C4 −0.7 (6) C19—C14—C15—C16 −2.6 (7)
C5—N1—C3—C4 178.9 (5) N2—C14—C15—C16 173.9 (4)
N1—C3—C4—N2 0.5 (7) C19—C14—C15—C20 176.5 (4)
C2—N2—C4—C3 −0.1 (7) N2—C14—C15—C20 −7.0 (7)
C14—N2—C4—C3 −177.3 (5) C14—C15—C16—C17 0.5 (7)
C2—N1—C5—C10 90.0 (6) C20—C15—C16—C17 −178.6 (5)
C3—N1—C5—C10 −89.4 (6) C15—C16—C17—C18 2.0 (7)
C2—N1—C5—C6 −97.3 (6) C15—C16—C17—C21 −175.3 (4)
C3—N1—C5—C6 83.2 (6) C16—C17—C18—C19 −2.6 (7)
C10—C5—C6—C7 −5.0 (7) C21—C17—C18—C19 174.7 (4)
N1—C5—C6—C7 −177.2 (4) C17—C18—C19—C14 0.6 (6)
C10—C5—C6—C11 172.9 (5) C17—C18—C19—C22 −178.4 (4)
N1—C5—C6—C11 0.7 (7) C15—C14—C19—C18 2.1 (6)
C5—C6—C7—C8 1.9 (8) N2—C14—C19—C18 −174.5 (4)
C11—C6—C7—C8 −176.1 (5) C15—C14—C19—C22 −178.9 (4)
C6—C7—C8—C9 0.4 (9) N2—C14—C19—C22 4.5 (6)
C6—C7—C8—C12 −179.0 (6)