| Oxford Diffraction Xcalibur E diffractometer | 2814 reflections with I > 2σ(I) |
| Radiation source: sealed tube | Rint = 0.049 |
| ω scans | θmax = 28.7°, θmin = 3.0° |
| Absorption correction: multi-scan (CrysAlis PRO; Agilent, 2014) | h = −14→14 |
| Tmin = 0.993, Tmax = 1.000 | k = −18→16 |
| 10241 measured reflections | l = −19→19 |
| 4960 independent reflections |