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. 2018 Aug 31;74(Pt 9):1369–1372. doi: 10.1107/S205698901801201X

Table 2. Experimental details.

Crystal data
Chemical formula [Cu2Cl4(C22H26N2O)2]
M r 937.77
Crystal system, space group Monoclinic, P21/n
Temperature (K) 123
a, b, c (Å) 11.1962 (8), 13.5321 (10), 15.5615 (8)
β (°) 107.705 (6)
V3) 2246.0 (3)
Z 2
Radiation type Mo Kα
μ (mm−1) 1.23
Crystal size (mm) 0.10 × 0.08 × 0.05
 
Data collection
Diffractometer Oxford Diffraction Xcalibur E
Absorption correction Multi-scan (CrysAlis PRO; Agilent, 2014)
T min, T max 0.993, 1.000
No. of measured, independent and observed [I > 2σ(I)] reflections 10241, 4960, 2814
R int 0.049
(sin θ/λ)max−1) 0.676
 
Refinement
R[F 2 > 2σ(F 2)], wR(F 2), S 0.062, 0.144, 1.05
No. of reflections 4960
No. of parameters 259
H-atom treatment H-atom parameters constrained
Δρmax, Δρmin (e Å−3) 0.43, −0.32

Computer programs: CrysAlis PRO (Agilent, 2014), SIR92 (Altomare et al., 1994), SHELXL2014 (Sheldrick, 2015) and Mercury (Macrae et al., 2008).