Bruker SMART CCD diffractometer | 2301 independent reflections |
Radiation source: fine-focus sealed tube | 1444 reflections with I > 3σ(I) |
Graphite monochromator | Rint = 0.040 |
ω scans | θmax = 25.0°, θmin = 2.5° |
Absorption correction: multi-scan (SADABS; Bruker, 2002) | h = −9→9 |
Tmin = 0.959, Tmax = 0.986 | k = −7→7 |
3523 measured reflections | l = −16→12 |