Bruker Kappa APEXII CCD diffractometer | 6717 independent reflections |
Radiation source: fine-focus sealed tube | 4398 reflections with I > 3σ(I) |
Graphite monochromator | Rint = 0.030 |
ω and φ scan | θmax = 32.6°, θmin = 1.8° |
Absorption correction: multi-scan (SADABS; Bruker, 2004) | h = −12→12 |
Tmin = 0.955, Tmax = 0.964 | k = −15→15 |
24261 measured reflections | l = −19→16 |