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. 2018 Aug 24;74(Pt 9):1344–1357. doi: 10.1107/S2056989018011544
Bruker Kappa APEXII CCD diffractometer 6717 independent reflections
Radiation source: fine-focus sealed tube 4398 reflections with I > 3σ(I)
Graphite monochromator Rint = 0.030
ω and φ scan θmax = 32.6°, θmin = 1.8°
Absorption correction: multi-scan (SADABS; Bruker, 2004) h = −12→12
Tmin = 0.955, Tmax = 0.964 k = −15→15
24261 measured reflections l = −19→16