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. 2018 Aug 24;74(Pt 9):1344–1357. doi: 10.1107/S2056989018011544
O1—C8 1.347 (3) C13—C14 1.415 (4)
O1—H1aa 0.7585 (19) C13—C18 1.415 (3)
O2—C17 1.359 (3) C14—H14a 0.93
O2—H2aa 0.922 (2) C14—C15 1.361 (4)
N1—C1 1.344 (4) C15—H15a 0.93
N1—C9 1.365 (3) C15—C16 1.406 (3)
N2—C10 1.325 (4) C16—H16a 0.93
N2—C18 1.371 (4) C16—C17 1.365 (4)
C1—H1a 0.93 C17—C18 1.429 (5)
C1—C2 1.392 (4) O3—C22 1.333 (3)
C2—H2a 0.93 O3—H3b 1.040 (2)
C2—C3 1.364 (4) O4—N3 1.227 (3)
C3—H3a 0.93 O5—N3 1.219 (3)
C3—C4 1.419 (4) O6—N4 1.226 (3)
C4—C5 1.418 (4) O7—N4 1.215 (3)
C4—C9 1.423 (4) O8—C25 1.242 (3)
C5—H5a 0.93 O9—C25 1.275 (3)
C5—C6 1.362 (4) O9—H3b 1.4952 (19)
C6—H6a 0.93 N3—C19 1.458 (3)
C6—C7 1.408 (4) N4—C21 1.473 (3)
C7—H7a 0.93 C19—C20 1.385 (4)
C7—C8 1.367 (4) C19—C24 1.388 (4)
C8—C9 1.433 (4) C20—H20a 0.93
C10—H10a 0.93 C20—C21 1.373 (3)
C10—C11 1.408 (4) C21—C22 1.408 (4)
C11—H11a 0.93 C22—C23 1.419 (3)
C11—C12 1.354 (4) C23—C24 1.394 (3)
C12—H12a 0.93 C23—C25 1.508 (4)
C12—C13 1.416 (4) C24—H24a 0.93
C8—O1—H1aa 118.2 (2) C13—C14—C15 120.2 (2)
C17—O2—H2aa 111.60 (19) H14a—C14—C15 119.88
C1—N1—C9 118.3 (2) C14—C15—H15a 119.61
C10—N2—C18 118.4 (2) C14—C15—C16 120.8 (2)
N1—C1—H1a 118.43 H15a—C15—C16 119.61
N1—C1—C2 123.1 (2) C15—C16—H16a 119.71
H1a—C1—C2 118.43 C15—C16—C17 120.6 (2)
C1—C2—H2a 120.19 H16a—C16—C17 119.71
C1—C2—C3 119.6 (3) O2—C17—C16 123.8 (2)
H2a—C2—C3 120.19 O2—C17—C18 116.0 (2)
C2—C3—H3a 120.26 C16—C17—C18 120.2 (2)
C2—C3—C4 119.5 (2) N2—C18—C13 121.8 (3)
H3a—C3—C4 120.27 N2—C18—C17 119.6 (2)
C3—C4—C5 122.8 (2) C13—C18—C17 118.6 (2)
C3—C4—C9 117.8 (2) C22—O3—H3b 102.89 (19)
C5—C4—C9 119.5 (2) C25—O9—H3b 102.84 (17)
C4—C5—H5a 120 O4—N3—O5 124.3 (2)
C4—C5—C6 120.0 (2) O4—N3—C19 117.5 (2)
H5a—C5—C6 120 O5—N3—C19 118.2 (2)
C5—C6—H6a 119.4 O6—N4—O7 124.2 (2)
C5—C6—C7 121.2 (2) O6—N4—C21 116.66 (19)
H6a—C6—C7 119.4 O7—N4—C21 119.1 (2)
C6—C7—H7a 119.72 N3—C19—C20 118.7 (2)
C6—C7—C8 120.6 (2) N3—C19—C24 118.9 (2)
H7a—C7—C8 119.72 C20—C19—C24 122.3 (2)
O1—C8—C7 123.5 (2) C19—C20—H20a 121.04
O1—C8—C9 116.5 (2) C19—C20—C21 117.9 (2)
C7—C8—C9 120.0 (2) H20a—C20—C21 121.04
N1—C9—C4 121.7 (2) N4—C21—C20 116.7 (2)
N1—C9—C8 119.6 (2) N4—C21—C22 120.67 (19)
C4—C9—C8 118.7 (2) C20—C21—C22 122.7 (2)
N2—C10—H10a 118.33 O3—C22—C21 122.3 (2)
N2—C10—C11 123.3 (2) O3—C22—C23 120.0 (2)
H10a—C10—C11 118.33 C21—C22—C23 117.7 (2)
C10—C11—H11a 120.58 C22—C23—C24 120.0 (2)
C10—C11—C12 118.8 (3) C22—C23—C25 120.6 (2)
H11a—C11—C12 120.58 C24—C23—C25 119.4 (2)
C11—C12—H12a 119.87 C19—C24—C23 119.2 (2)
C11—C12—C13 120.3 (2) C19—C24—H24a 120.38
H12a—C12—C13 119.87 C23—C24—H24a 120.38
C12—C13—C14 123.1 (2) O8—C25—O9 125.0 (2)
C12—C13—C18 117.4 (2) O8—C25—C23 118.9 (2)
C14—C13—C18 119.6 (3) O9—C25—C23 116.1 (2)
C13—C14—H14a 119.88 O3—H3b—O9 155.88 (12)