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. 2018 Aug 24;74(Pt 9):1344–1357. doi: 10.1107/S2056989018011544
Bruker SMART APEXII CCD area-detector diffractometer 4061 independent reflections
Radiation source: fine-focus sealed tube 3042 reflections with I > 3σ(I)
Graphite monochromator Rint = 0.030
φ and ω scans θmax = 27.5°, θmin = 1.7°
Absorption correction: multi-scan (SADABS; Bruker, 2009) h = −8→8
Tmin = 0.937, Tmax = 0.987 k = −14→12
17014 measured reflections l = −15→15