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. 2018 Aug 24;74(Pt 9):1344–1357. doi: 10.1107/S2056989018011544
O1—C1 1.2939 (17) C4—C5 1.3881 (18)
O1—H7 1.4329 (9) C5—H5a 0.93
O2—N2 1.2279 (17) C5—C6 1.3816 (19)
O3—N2 1.2346 (17) C6—C7 1.4844 (18)
O4—N1 1.2304 (15) C8—C9 1.439 (2)
O5—N1 1.2321 (15) C9—H9a 0.93
O6—C7 1.2355 (16) C9—C10 1.3449 (19)
O7—C7 1.3040 (17) C10—C15 1.4889 (19)
O7—H7 1.0191 (9) C11—C12 1.4936 (19)
O8—C8 1.2198 (17) C12—H12a 0.98
N1—C4 1.4597 (18) C12—C13 1.531 (2)
N2—C2 1.4576 (17) C12—C14 1.5318 (19)
N3—C10 1.3963 (18) C13—H13a 0.96
N3—C11 1.3236 (17) C13—H13b 0.96
N3—H1n3 0.9729 (11) C13—H13c 0.96
N4—C8 1.4152 (18) C14—H14a 0.96
N4—C11 1.3303 (17) C14—H14b 0.96
N4—H1n4 0.9085 (11) C14—H14c 0.96
C1—C2 1.4259 (18) C15—H15a 0.96
C1—C6 1.4349 (19) C15—H15b 0.96
C2—C3 1.381 (2) C15—H15c 0.96
C3—H3a 0.93 O1w—H2w1 0.9169 (10)
C3—C4 1.3763 (19) O1w—H1w1 0.9146 (10)
C1—O1—H7 96.54 (8) N4—C8—C9 113.60 (12)
C7—O7—H7 101.27 (9) C8—C9—H9a 119.24
O4—N1—O5 124.04 (12) C8—C9—C10 121.51 (13)
O4—N1—C4 118.12 (11) H9a—C9—C10 119.24
O5—N1—C4 117.84 (11) N3—C10—C9 118.95 (12)
O2—N2—O3 123.42 (12) N3—C10—C15 116.00 (11)
O2—N2—C2 119.16 (12) C9—C10—C15 125.06 (13)
O3—N2—C2 117.39 (12) N3—C11—N4 118.76 (12)
C10—N3—C11 122.45 (11) N3—C11—C12 120.45 (12)
C10—N3—H1n3 118.37 (11) N4—C11—C12 120.78 (12)
C11—N3—H1n3 119.14 (11) C11—C12—H12a 108.71
C8—N4—C11 124.69 (12) C11—C12—C13 109.61 (13)
C8—N4—H1n4 116.55 (11) C11—C12—C14 111.42 (10)
C11—N4—H1n4 118.72 (12) H12a—C12—C13 108.78
O1—C1—C2 124.06 (12) H12a—C12—C14 106.87
O1—C1—C6 120.40 (11) C13—C12—C14 111.36 (12)
C2—C1—C6 115.53 (12) C12—C13—H13a 109.47
N2—C2—C1 120.85 (12) C12—C13—H13b 109.47
N2—C2—C3 116.56 (11) C12—C13—H13c 109.47
C1—C2—C3 122.58 (12) H13a—C13—H13b 109.47
C2—C3—H3a 120.52 H13a—C13—H13c 109.47
C2—C3—C4 118.97 (12) H13b—C13—H13c 109.47
H3a—C3—C4 120.52 C12—C14—H14a 109.47
N1—C4—C3 118.77 (12) C12—C14—H14b 109.47
N1—C4—C5 119.38 (12) C12—C14—H14c 109.47
C3—C4—C5 121.85 (13) H14a—C14—H14b 109.47
C4—C5—H5a 120.33 H14a—C14—H14c 109.47
C4—C5—C6 119.34 (12) H14b—C14—H14c 109.47
H5a—C5—C6 120.33 C10—C15—H15a 109.47
C1—C6—C5 121.71 (12) C10—C15—H15b 109.47
C1—C6—C7 119.30 (12) C10—C15—H15c 109.47
C5—C6—C7 118.99 (12) H15a—C15—H15b 109.47
O6—C7—O7 122.20 (12) H15a—C15—H15c 109.47
O6—C7—C6 121.26 (12) H15b—C15—H15c 109.47
O7—C7—C6 116.54 (12) H2w1—O1w—H1w1 110.00 (10)
O8—C8—N4 119.14 (12) O1—H7—O7 165.94 (7)
O8—C8—C9 127.26 (13)