Bruker APEXII CCD diffractometer | 7344 independent reflections |
Radiation source: fine-focus sealed tube | 5724 reflections with I > 3σ(I) |
Graphite monochromator | Rint = 0.015 |
φ and ω scans | θmax = 28.3°, θmin = 2.0° |
Absorption correction: multi-scan (SADABS; Bruker, 2008) | h = −19→19 |
Tmin = 0.932, Tmax = 1.000 | k = −17→17 |
29552 measured reflections | l = −21→15 |