Skip to main content
. 2018 Aug 24;74(Pt 9):1344–1357. doi: 10.1107/S2056989018011544
Bruker APEX DUO CCD area-detector diffractometer 4943 independent reflections
Radiation source: fine-focus sealed tube 3677 reflections with I > 3σ(I)
Graphite monochromator Rint = 0.023
φ and ω scans θmax = 32.5°, θmin = 1.3°
Absorption correction: multi-scan (SADABS; Bruker, 2009) h = −8→8
Tmin = 0.963, Tmax = 0.990 k = −12→11
12709 measured reflections l = −22→23