Bruker APEX DUO CCD area-detector diffractometer | 4943 independent reflections |
Radiation source: fine-focus sealed tube | 3677 reflections with I > 3σ(I) |
Graphite monochromator | Rint = 0.023 |
φ and ω scans | θmax = 32.5°, θmin = 1.3° |
Absorption correction: multi-scan (SADABS; Bruker, 2009) | h = −8→8 |
Tmin = 0.963, Tmax = 0.990 | k = −12→11 |
12709 measured reflections | l = −22→23 |