Table 2. NMR peak assignments of pure disodium (R/S)-2-hydroxyglutarate at pH 7.0.
Assignment | 1H shift (ppm, with multiplicity) | 13C shift (ppm) |
---|---|---|
1COOH | - | 184.2 |
2CH(OH) | 4.02 (q) | 75.0 |
3CH2 | 2.00 (m), 1.84 (m) | 33.9 |
4CH2 | 2.29 (m), 2.24 (m) | 36.4 |
5COOH | - | 185.8 |
Note. ppm = parts per million, q = quartet, m = other multiplet